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NMR of Quadrupolar Nuclei in Solid Materials (Emr Books)

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NMR of Quadrupolar Nuclei in Solid Materials (Emr Books) Cover

 

Synopses & Reviews

Publisher Comments:

The content of this volume has been added to eMagRes (formerly Encyclopedia of Magnetic Resonance) - the ultimate online resource for NMR and MRI.

Over the past 20 years technical developments in superconducting magnet technology and instrumentation have increased the potential of NMR spectroscopy so that it is now possible to study a wide range of solid materials. In addition, one can probe the nuclear environments of many other additional atoms that possess the property of spin. In particular, it is possible to carry out NMR experiments on isotopes that have nuclear spin greater that ½ (i.e.  quadrupolar nuclei). Since more that two-thirds of all NMR active isotopes are quadrupolar nuclei, applications of NMR spectroscopy with quadrupolar nuclei are increasing rapidly.

The purpose of this handbook is to provide under a single cover the fundamental principles, techniques and applications of quadrupolar NMR as it pertains to solid materials. Each chapter has been prepared by an expert who has made significant contributions to out understanding and appreciation of the importance of NMR studies of quadrupolar nuclei in solids. The text is divided into three sections: The first provides the reader with the background necessary to appreciate the challenges in acquiring and interpreting NMR spectra of quadrupolar neclei in solids. The second presents cutting-edge techniques and methodology for employing these techniques to investigate quadrupolar nuclei in solids. The final section explores applications of solid-state NMR studies of solids ranging from investigations of dynamics, characterizations of biological samples, organic and inorganic materials, porous materials, glasses, catalysts, semiconductors and high-temperature superconductors.

About EMR Handbooks / eMagRes Handbooks 

The Encyclopedia of Magnetic Resonance (up to 2012) and eMagRes (from 2013 onward) publish a wide range of online articles on all aspects of magnetic resonance in physics, chemistry, biology and medicine. The existence of this large number of articles, written by experts in various fields, is enabling the publication of a series of EMR Handbooks / eMagRes Handbooks on specific areas of NMR and MRI. The chapters of each of these handbooks will comprise a carefully chosen selection of articles from eMagRes. In consultation with the eMagRes Editorial Board, the EMR Handbooks / eMagRes Handbooks  are coherently planned in advance by specially-selected Editors, and new articles are written (together with updates of some already existing articles) to give appropriate complete coverage. The handbooks are intended to be of value and interest to research students, postdoctoral fellows and other researchers learning about the scientific area in question and undertaking relevant experiments, whether in academia or industry.

Have the content of this Handbook and the complete content of eMagRes at your fingertips!
Visit: www.wileyonlinelibrary.com/ref/eMagRes

View other eMagRes publications here

Synopsis:

Over the past 20 years technical developments in superconducting magnet technology and instrumentation have increased the potential of NMR spectroscopy so that it is now possible to study a wide range of solid materials. In addition, one can probe the nuclear environments of many other additional atoms that possess the property of spin. In particular, it is possible to carry out NMR experiments on isotopes that have nuclear spin greater that ½ (i.e.  quadrupolar nuclei). Since more that two-thirds of all NMR active isotopes are quadrupolar nuclei, applications of NMR spectroscopy with quadrupolar nuclei are increasing rapidly.

The purpose of this handbook is to provide under a single cover the fundamental principles, techniques and applications of quadrupolar NMR as it pertains to solid materials. Each chapter has been prepared by an expert who has made significant contributions to out understanding and appreciation of the importance of NMR studies of quadrupolar nuclei in solids. The text is divided into three sections: The first provides the reader with the background necessary to appreciate the challenges in acquiring and interpreting NMR spectra of quadrupolar neclei in solids. The second presents cutting-edge techniques and methodology for employing these techniques to investigate quadrupolar nuclei in solids. The final section explores applications of solid-state NMR studies of solids ranging from investigations of dynamics, characterizations of biological samples, organic and inorganic materials, porous materials, glasses, catalysts, semiconductors and high-temperature superconductors.

About EMR Handbooks

The Encyclopedia of Magnetic Resonance (EMR) publishes a wide range of online articles on all aspects of magnetic resonance in physics, chemistry, biology and medicine. The existence-of this large number of articles, written by experts in various fields, is enabling the publication of a series of EMR Handbooks on specific areas of NMR and MRI. The chapters of each of these handbooks will comprise a carefully chosen selection of Encyclopedia articles. In consultation wit the EMR Editorial Board, the EMR Handbooks are coherently planned in advance by specially-selected Editors, and new articles, are written (together with updates of some already existing articles) to give appropriate complete coverage. The handbooks are intended to be of value and interest to research students, postdoctoral  fellows and other researchers learning about the scientific area in question and undertaking relevant experiments, whether in academia or industry.

Have the content of this handbook and the complete content of the Encyclopedia of Magnetic Resonance at your fingertips! Visit: www.wileyonlinelibrary.com/ref/emr

Synopsis:

Many important materials do not contain spin-1/2 nuclei traditionally investigated by NMR spectroscopy and secondly, dissolving solid materials in a solvent may be impossible or may destroy the integrity of the material.  All these obstacles can be overcome by NMR experiments at high-magnetic field strengths and investigating the properties of quadrupolar nuclei.

This Handbook gives an up-to-date account of NMR of quadrupoloar nuclei in the solid state. Each chapter of the Handbook has been prepared by an expert who has made significant contributions to our understanding and appreciation of the importance of NMR studies of quadrupolar nuclei in solids. The text is divided into three Parts:  A) Basic Principles of Quadrupolar NMR, B) Advanced Solid-State NMR Techniques to Investigate Quadrupolar Nuclei and C) Applications Involving NMR Studies of Quadrupolar Nuclei in Solids.

The first section provides the reader with the background necessary to appreciate the challenges in acquiring and interpreting NMR spectra of quadrupolar nuclei in solids. The second section presents cutting-edge techniques and methodology for employing these spectroscopic techniques to investigate quadrupolar nuclei in solids. The final section explores applications of solid-state NMR studies of solids ranging from investigations of biological samples to porous materials, catalysts, geological samples and high-temperature superconductors. 

All these articles will be published on EMR:  http://onlinelibrary.wiley.com/book/10.1002/9780470034590

Table of Contents

Basic Principles of Quadrupolar NMR

Quadrupolar Interactions

Quadrupolar Nuclei in Solids

Quadrupolar Coupling: An Introduction and Crystallographic Aspects

Quadrupolar Nuclei in Solids:  Influence of different interactions on spectra

Advanced Solid-State NMR Techniques to Investigate Quadrupolar Nuclei

Acquisition of Wideline Solid-State NMR Spectra of Quadrupolar Nuclei

Sensitivity and Resolution Enhancement of Half-Integer Quadrupolar Nuclei in Solid-State NMR

Quadrupolar Nutation Spectroscopy

Dynamic Angle Spinning

DOuble Rotation (DOR) NMR

MQMAS NMR: Experimental Strategies

STMAS NMR: Experimental Advances

Correlation Experiments involving Half-Integer Quadrupolar Nuclei

Computing Electric Field Gradient Tensors

Applications Involving NMR Studies of Quadrupolar Nuclei in Solids

Quadrupolar NMR to Investigate Dynamics in Solid Materials

Alkali Metal NMR of Biological Molecules

Nitrogen-14 NMR Studies of Biological Systems

Oxygen-17 NMR Studies of Organic and Biological Molecules

Oxygen-17 NMR of Inorganic Materials

Chlorine, Bromine and Iodine Solid-State NMR

Quadrupolar NMR of Ionic Conductors, Batteries, and other Energy-Related Materials

Quadrupolar NMR of Nanoporous Materials

Quadrupolar NMR in the Earth Sciences

Quadrupolar NMR of Superconductors

Quadrupolar NMR of Semiconductors

Quadrupolar NMR of Metal Nuclides in Biological Materials

Nuclear Waste Glasses: Insights from Solid-State NMR

Quadrupolar Metal NMR of Oxide Materials Including Catalysts

Quadrupolar NMR of Intermetallic Compounds

Product Details

ISBN:
9780470973981
Author:
Wasylishen, Roderick E.
Publisher:
Wiley
Author:
Wimperis, Stephen
Author:
Prof Sharon Ashbrook
Author:
Ashbrook, Sharon E.
Author:
Ashbrook, Sharon
Author:
Prof Stephen Wimperis
Subject:
Spectrum Analysis
Subject:
NMR Spectroscopy / MRI / Imaging
Subject:
Physics-Spectroscopy
Copyright:
Series:
eMagRes Books
Series Volume:
3
Publication Date:
20120416
Binding:
Electronic book text in proprietary or open standard format
Language:
English
Pages:
550
Dimensions:
229 x 152 mm

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Science and Mathematics » Physics » Spectroscopy

NMR of Quadrupolar Nuclei in Solid Materials (Emr Books) New Hardcover
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Product details 550 pages John Wiley & Sons - English 9780470973981 Reviews:
"Synopsis" by , Over the past 20 years technical developments in superconducting magnet technology and instrumentation have increased the potential of NMR spectroscopy so that it is now possible to study a wide range of solid materials. In addition, one can probe the nuclear environments of many other additional atoms that possess the property of spin. In particular, it is possible to carry out NMR experiments on isotopes that have nuclear spin greater that ½ (i.e.  quadrupolar nuclei). Since more that two-thirds of all NMR active isotopes are quadrupolar nuclei, applications of NMR spectroscopy with quadrupolar nuclei are increasing rapidly.

The purpose of this handbook is to provide under a single cover the fundamental principles, techniques and applications of quadrupolar NMR as it pertains to solid materials. Each chapter has been prepared by an expert who has made significant contributions to out understanding and appreciation of the importance of NMR studies of quadrupolar nuclei in solids. The text is divided into three sections: The first provides the reader with the background necessary to appreciate the challenges in acquiring and interpreting NMR spectra of quadrupolar neclei in solids. The second presents cutting-edge techniques and methodology for employing these techniques to investigate quadrupolar nuclei in solids. The final section explores applications of solid-state NMR studies of solids ranging from investigations of dynamics, characterizations of biological samples, organic and inorganic materials, porous materials, glasses, catalysts, semiconductors and high-temperature superconductors.

About EMR Handbooks

The Encyclopedia of Magnetic Resonance (EMR) publishes a wide range of online articles on all aspects of magnetic resonance in physics, chemistry, biology and medicine. The existence-of this large number of articles, written by experts in various fields, is enabling the publication of a series of EMR Handbooks on specific areas of NMR and MRI. The chapters of each of these handbooks will comprise a carefully chosen selection of Encyclopedia articles. In consultation wit the EMR Editorial Board, the EMR Handbooks are coherently planned in advance by specially-selected Editors, and new articles, are written (together with updates of some already existing articles) to give appropriate complete coverage. The handbooks are intended to be of value and interest to research students, postdoctoral  fellows and other researchers learning about the scientific area in question and undertaking relevant experiments, whether in academia or industry.

Have the content of this handbook and the complete content of the Encyclopedia of Magnetic Resonance at your fingertips! Visit: www.wileyonlinelibrary.com/ref/emr

"Synopsis" by , Many important materials do not contain spin-1/2 nuclei traditionally investigated by NMR spectroscopy and secondly, dissolving solid materials in a solvent may be impossible or may destroy the integrity of the material.  All these obstacles can be overcome by NMR experiments at high-magnetic field strengths and investigating the properties of quadrupolar nuclei.

This Handbook gives an up-to-date account of NMR of quadrupoloar nuclei in the solid state. Each chapter of the Handbook has been prepared by an expert who has made significant contributions to our understanding and appreciation of the importance of NMR studies of quadrupolar nuclei in solids. The text is divided into three Parts:  A) Basic Principles of Quadrupolar NMR, B) Advanced Solid-State NMR Techniques to Investigate Quadrupolar Nuclei and C) Applications Involving NMR Studies of Quadrupolar Nuclei in Solids.

The first section provides the reader with the background necessary to appreciate the challenges in acquiring and interpreting NMR spectra of quadrupolar nuclei in solids. The second section presents cutting-edge techniques and methodology for employing these spectroscopic techniques to investigate quadrupolar nuclei in solids. The final section explores applications of solid-state NMR studies of solids ranging from investigations of biological samples to porous materials, catalysts, geological samples and high-temperature superconductors. 

All these articles will be published on EMR:  http://onlinelibrary.wiley.com/book/10.1002/9780470034590

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