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Spectrometric Identification of Organic Compounds

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Spectrometric Identification of Organic Compounds Cover

 

Synopses & Reviews

Publisher Comments:

Originally published in 1962, this was the first book to explore teh identification of organic compounds using spectroscopy. It provides a thorough introduction to the three areas of spectrometry most widely used in spectrometric identification: mass spectrometry, infrared spectrometry, and nuclear magnetic resonance spectrometry. A how-to, hands-on teaching manual with considerably expanded NMR coverage--NMR spectra can now be intrepreted in exquisite detail. This book:

* Uses a problem-solving approach with extensive reference charts and tables.

* Offers an extensive set of real-data problems offers a challenge to the practicing chemist

Table of Contents

Chapter 1. Mass Spectrometry.

1.1 Introduction.

1.2 Instrumentation.

1.3 Ionization Methods.

1.4 Mass Analyzers.

1.5 Interpretation of El Mass Spectra.

1.6 Mass Spectra of Some Chemical Classes.

Chapter 2. Infrared Spectrometry.

2.1 Introduction.

2.2 Theory.

2.3 Instrumentation.

2.4 Sample Handling.

2.5 Interpretations of Spectra.

2.6 Characteristic Group Absorption of Organic Molecules.

Chapter 3. Proton Magnetic Resonance Spectrometry.

3.1 Introduction.

3.2 Theory.

3.3 Instrumentation and Sample Handling.

3.4 Chemical Shift.

3.5 Spin Coupling, Multiplets, Spin Systems.

3.6 Protons on Oxygen, Nitrogen, and Sulfur Atoms. Exchangeable Protons.

3.7 Coupling of Protons to Other Important Nuclei (<sup>19</sup>F, E, <sup>31</sup>P, <sup>29</sup>Si, and <sup>13</sup>C.

3.8 Chemical Shift Equivalence.

3.9 Magnetic Equivalence (Spin-Coupling Equivalence).

3.10 AMX, ABX, and ABC Rigid Systems with Three Coupling Constants.

3.11 Confirmationally Mobile, Open-Chain Systems. Virtual Coupling.

3.12 Chirality.

3.13 Vicinal and Geminal Coupling.

3.14 Low-Range Coupling.

3.15 Selective Spin Decoupling. Double Resonance.

3.16 Nuclear Overhauser Effect, Difference Spectrometry, 1H 1H Proximity Through Space.

Chapter 4. Carbon-13 NMR Spectrometry.

4.1 Introduction.

4.2 Theory.

4.3 Interpretation of a Simple <sup>13</sup>C Spectrum: Diethyl Phthalate.

4.4 Quantitative <sup>13</sup>C Analysis.

4.5 Chemical Shift Equivalence.

4.6 DEPT.

4.7 Chemical Classes and Chemical Shifts.

Chapter 5. Correlation NMR Spectrometry; 2-D NMR.

5.1 Introduction.

5.2 Theory.

5.3 Correlation Spectrometry.

5.4 Ipsenol: <sup>1</sup>H-<sup>1</sup>H COSY.

5.5 Caryophyllene Oxide.

5.6 <sup>13</sup>C-<sup>13</sup>C Correlations: Inadequate.

5.7 Lactose.

5.8 Relayed Coherence Transfer: TOCSY.

5.9 HMQC – TOCSY.

5.10 ROESY.

5.11 VGSE.

5.12 Gradient Field NMR.

Chapter 6. NMR Spectrometry of Other Important Spin 1/2 Nuclei.

6.1 Introduction.

6.2 <sup>15</sup>N Nuclear Magnetic Resonance.

6.3 <sup>19</sup>F Nuclear Magnetic Resonance.

6.4 <sup>29</sup>Si Nuclear Magnetic Resonance.

6.5 <sup>31</sup>P Nuclear Magnetic Resonance.

6.6 Conclusion.

Chapter 7. Solved Problems.

7.1 Introduction.

Chapter 8. Assigned Problems.

8.1 Introduction.

Product Details

ISBN:
9780471393627
Author:
Silverstein, Robert M.
Author:
Kiemle, David
Author:
Webster, Francis X.
Publisher:
John Wiley & Sons
Subject:
Chemistry - Organic
Subject:
Chemistry - Analytic
Subject:
Chemistry - Physical & Theoretical
Subject:
Spectrum Analysis
Subject:
Organic compounds
Subject:
Spectroscopy & Spectrum Analysis
Subject:
Organic compounds -- Spectra.
Subject:
Physics-Spectroscopy
Subject:
Spectroscopy
Copyright:
Edition Number:
7
Publication Date:
January 2005
Binding:
HARDCOVER
Grade Level:
College/higher education:
Language:
English
Illustrations:
Y
Pages:
512
Dimensions:
282 x 224 x 25 mm 43.2 oz

Related Subjects

Health and Self-Help » Health and Medicine » General
Health and Self-Help » Health and Medicine » General Medicine
Reference » Science Reference » General
Science and Mathematics » Chemistry » Analytical
Science and Mathematics » Chemistry » Organic
Science and Mathematics » Chemistry » Physical Chemistry
Science and Mathematics » Physics » Spectroscopy
Textbooks » General

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