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Spectrometric Identification of Organic Compoundsby Robert M. Silverstein
Synopses & Reviews
Originally published in 1962, this was the first book to explore teh identification of organic compounds using spectroscopy. It provides a thorough introduction to the three areas of spectrometry most widely used in spectrometric identification: mass spectrometry, infrared spectrometry, and nuclear magnetic resonance spectrometry. A how-to, hands-on teaching manual with considerably expanded NMR coverage--NMR spectra can now be intrepreted in exquisite detail. This book:
* Uses a problem-solving approach with extensive reference charts and tables.
* Offers an extensive set of real-data problems offers a challenge to the practicing chemist
Table of Contents
Chapter 1. Mass Spectrometry.
1.3 Ionization Methods.
1.4 Mass Analyzers.
1.5 Interpretation of El Mass Spectra.
1.6 Mass Spectra of Some Chemical Classes.
Chapter 2. Infrared Spectrometry.
2.4 Sample Handling.
2.5 Interpretations of Spectra.
2.6 Characteristic Group Absorption of Organic Molecules.
Chapter 3. Proton Magnetic Resonance Spectrometry.
3.3 Instrumentation and Sample Handling.
3.4 Chemical Shift.
3.5 Spin Coupling, Multiplets, Spin Systems.
3.6 Protons on Oxygen, Nitrogen, and Sulfur Atoms. Exchangeable Protons.
3.7 Coupling of Protons to Other Important Nuclei (<sup>19</sup>F, E, <sup>31</sup>P, <sup>29</sup>Si, and <sup>13</sup>C.
3.8 Chemical Shift Equivalence.
3.9 Magnetic Equivalence (Spin-Coupling Equivalence).
3.10 AMX, ABX, and ABC Rigid Systems with Three Coupling Constants.
3.11 Confirmationally Mobile, Open-Chain Systems. Virtual Coupling.
3.13 Vicinal and Geminal Coupling.
3.14 Low-Range Coupling.
3.15 Selective Spin Decoupling. Double Resonance.
3.16 Nuclear Overhauser Effect, Difference Spectrometry, 1H 1H Proximity Through Space.
Chapter 4. Carbon-13 NMR Spectrometry.
4.3 Interpretation of a Simple <sup>13</sup>C Spectrum: Diethyl Phthalate.
4.4 Quantitative <sup>13</sup>C Analysis.
4.5 Chemical Shift Equivalence.
4.7 Chemical Classes and Chemical Shifts.
Chapter 5. Correlation NMR Spectrometry; 2-D NMR.
5.3 Correlation Spectrometry.
5.4 Ipsenol: <sup>1</sup>H-<sup>1</sup>H COSY.
5.5 Caryophyllene Oxide.
5.6 <sup>13</sup>C-<sup>13</sup>C Correlations: Inadequate.
5.8 Relayed Coherence Transfer: TOCSY.
5.9 HMQC – TOCSY.
5.12 Gradient Field NMR.
Chapter 6. NMR Spectrometry of Other Important Spin 1/2 Nuclei.
6.2 <sup>15</sup>N Nuclear Magnetic Resonance.
6.3 <sup>19</sup>F Nuclear Magnetic Resonance.
6.4 <sup>29</sup>Si Nuclear Magnetic Resonance.
6.5 <sup>31</sup>P Nuclear Magnetic Resonance.
Chapter 7. Solved Problems.
Chapter 8. Assigned Problems.
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